1. Kukho iikristale eziphezulu ze-conductivity kwiseli ye-conductivity.
Isisombululo: Emva kokucoca i-cell conductivity kunye ne-1: 1 nitric acid, yihlambulule ngamanzi adibeneyo.
2. I-eluent ayisulungekanga ngokwaneleyo.
Isixazululo: ukutshintsha imeko.
3. Ikholamu yechromatographic ifunxa izinto eziphezulu ze-conductivity.
Isisombululo: I-Washcolumn ngokuphindaphindiweyo kwaye ngokutshintshana kunye ne-eluent kunye namanzi.
4. Ukhetho olungalunganga lwesikali sokulinganisa
Xa kusenziwa uhlalutyo lwe-ion olulungileyo, njengoko i-conductivity yangasemva ye-eluate iphezulu kakhulu, ukukhethwa kwesikali sokulinganisa esisezantsi kakhulu kuya kukhokelela ekubonakalisweni kwexabiso eliphezulu kakhulu le-conductivity.Khetha nje isikali sokulinganisa kwakhona.
5. Umcinezeli akasebenzi
Isisombululo: Jonga ukuba isicinezeli siyasebenza na.
6. Uxinaniso lwesampulu luphezulu kakhulu.
Isisombululo: Nciphisa isampuli.
1. Kukho amaqamza kwimpompo.
Isisombululo: Ivalve yokukhupha ivalufa echasene newotshi, ivalve yokukhupha impompo, amaqamza aphumayo.
2. Ivalve yokutshekisha yempompo ingcolisekile okanye yonakele.
Isisombululo: Guqula ivalve yokukhangela okanye uyibeke kwi-1: 1 isisombululo se-nitric sokucoca nge-supersonic.
3. Isihluzo esikwibhotile ye-eluent singcolisekile okanye sivaliwe.
Isisombululo: Faka endaweni yesihluzi.
4. Ukukhutshwa kwegesi ngokwaneleyo kwe-eluent.
Isisombululo: Faka endaweni ye-eluent.
Isisombululo: Jonga indawo evalekileyo ecaleni kwendlela yokuhamba ukuze uchonge kwaye ucime ukuvaleka.
1. Inwebu yesihluzo sekholamu ivaliwe.
Isisombululo: Susa ikholamu kwaye ukhulule isiphelo sokungena.Thatha i-sieve plate ngononophelo, yifake kwi-1: 1 i-nitric acid kwaye uyihlambe nge-ultrasonic wave imizuzu engama-30, uze uyihlambulule ngamanzi adibeneyo kwaye uyihlanganisele kwakhona, ubuyisele ukudibanisa i-chromatograph yokucoca.Qaphela ukuba ichromatograph ayinakudityaniswa nendlela yokuhamba.
2. Ivalve eneendlela ezintandathu zokutofa ivalekile.
Isisombululo: Jonga indawo evalekileyo ecaleni kwendlela yokuhamba ukuze uchonge kwaye ulungise ingxaki.
3. Ivalve yokukhangela impompo ivaliwe.
Isisombululo: Guqula ivalve yokukhangela okanye uyibeke kwi-1: 1 isisombululo se-nitric sokucoca nge-supersonic.
4. Indlela yokuhamba ivaliwe.
Isisombululo: Fumana indawo yokuvala ngokwendlela yokuphelisa ngokuthe ngcembe kwaye wenze enye indawo.
5. Isantya esigqithisileyo.
Isisombululo: Lungisa impompo kwisantya esifanelekileyo sokuhamba.
6. Uxinzelelo oluphezulu lomda wempompo lubekwe phantsi kakhulu.
Isisombululo: Ngaphantsi kokuhamba komsebenzi wekholamu yechromatographic, lawula olona xinzelelo luphezulu lomda ukuba lube yi-5 MPa ngaphezu koxinzelelo olusebenzayo lwangoku.
1. Isixhobo asisebenzi ixesha elide ngokwaneleyo njengoko kucwangcisiwe.
Isisombululo:Ukufakwa rhoqo kwe-eluent de isixhobo sizinzile.
2. Kukho amaqamza kwimpompo.
Isisombululo: Ivalve yokukhupha ivalufa echasene newotshi, ivalve yokukhupha impompo, amaqamza aphumayo.
3. Isihluzo sombhobho wokungena kwamanzi wempompo sivaliwe, sivelise uxinzelelo olubi phantsi kwamandla okufunxa kunye nokuvelisa amaqamza.
Isisombululo: Ukutshintsha isihluzo okanye ukubeka isihluzo kwi-1: 1 1M i-nitric acid ukuze ihlanjwe i-5min kunye ne-ultrasonic bath.
4. Kukho amaqamza kwikholamu.
Isisombululo: Sebenzisa i-eluent elungiselelwe ngamanzi adibeneyo ukuhlambulula ikholamu ngesantya esiphantsi ukususa amaqamza.
5. Kukho amaqamza kwindlela yokuhamba.
Isisombululo: Susa ikholamu kunye nokukhupha amaqamza emanzini.
6. Kukho amaqamza kwi-cell conductivity, ebangela ukuguquguquka rhoqo kwesiseko.
Isisombululo: Ukugungxula i-conductivity cel, amaqamza adinayo
7. I-voltage ayizinzile okanye iphazamisekile kwi-static electrostatic.
Isisombululo: Yongeza i-voltage stabilizer kwaye usilalise isixhobo.
1. Ixesha lokufudumeza kwangaphambili kwesixhobo alanelanga.
Isisombululo: Yandisa ixesha lokufudumeza kwangaphambili.
2. Ukuvuza kokuhamba.
Isisombululo: Fumana indawo yokuvuza kwaye uyilungise, ukuba ayinakusonjululwa, buyisela indawo edibeneyo.
3. I-voltage ayizinzile okanye iphazamisekile kwi-static electrostatic.
Isisombululo: Yongeza i-voltage stabilizer kwaye usilalise isixhobo.
1. Ukugxininiswa kwe-eluent ayifanelekanga.
Isisombululo: Khetha ugxininiso olufanelekileyo .
2. Isantya sokuhamba kwe-eluentis siphezulu kakhulu.
Isisombululo: Khetha isantya esifanelekileyo sokuhamba kwe-eluent.
3. Ukusebenzisa iisampulu ezigxininise kakhulu
Isisombululo: Nciphisa isampuli.
4. Ikholamu ingcolisekile.
Isisombululo: Hlaziya okanye ubuyisele ikholamu.
1. Umthamo we-injection wesampuli awutshintshi.
Isisombululo: Tofa isampuli kumthamo ngaphezu kwamaxesha e-10 omthamo weringi yobungakanani ukuqinisekisa ukuba inaliti epheleleyo.
2. Ukugxininiswa kwesampuli esitofiweyo akufanelekanga.
Isisombululo: Khetha ugxininiso olululo lwesampulu etofiweyo.
3. I-reagent ayihlambulukanga.
Isisombululo: Faka indawo ye-reagent.
4. Izinto zangaphandle zikhona kumanzi adibeneyo.
Isisombululo: Faka endaweni yamanzi adiyoni.
5. Ukuhamba kuyatshintsha.
Isisombululo: Fumana izizathu zolo tshintsho kwaye ulungelelanise kwimeko yokuqala.
6. Indlela yokuhamba ivaliwe.
Isisombululo: fumana indawo evaliweyo, lungisa okanye wenze enye indawo.
1. I-reagent ayihlambulukanga.
Isisombululo: Tshintsha ii-reagents.
2. Amanzi adityanisiweyo aqulethe ukungcola.
Isisombululo: Faka endaweni yamanzi adiyoni.
1. Ufakelo olungalunganga lweseli conductivity.
Isisombululo: Faka kwakhona iseli ye-conductivity.
2. Iseli conductivity conductivity yonakele.
Isisombululo: Faka endaweni yeseli conductivity.
3. Ipompo ayinaso isisombululo sokuphuma.
Isisombululo: Jonga isalathisi soxinzelelo ukuze uqinisekise ukuba impompo isebenza.
1. Isisombululo esisemgangathweni singcolile, ngakumbi iisampuli eziphantsi.
Isisombululo: Lungisa kwakhona isisombululo.
2. Amanzi adityanisiweyo akacocekanga.
Isisombululo: buyisela amanzi adiyiniweyo.
3. Uxinzelelo lwesampulu luphezulu kakhulu okanye luphantsi kakhulu, ngaphandle koluhlu lomgca wesixhobo.
Isisombululo: Khetha uluhlu olufanelekileyo lokugxila.
Isisombululo: buyisela intambo yombane okanye unikezelo lwangoku lwangoku lwamandla.
1. Irhasi efunxekileyo kumbhobho wendlela yokuhamba
Isisombululo: xa unikezelo lwamanzi luvuliwe, vula ivalve yokukhupha yempompo, qalisa impompo yeplunger kwaye uhlale ungcangcazela isihluzo ukuze uyisuse ngokupheleleyo igesi.
2. Ubushushu obuphezulu kakhulu bangaphakathi obukhokelela ekukhutshweni kwegesi ngokwaneleyo kwamanzi adiyoni.
Isisombululo: Sebenzisa isixhobo sokukhupha umoya kwi-intanethi.
3. Ivalve yokutshekisha yempompo ingcolisekile okanye yonakele.
Isisombululo: Guqula ivalve yokukhangela okanye uyibeke kwi-1: 1 isisombululo se-nitric sokucoca nge-supersonic.